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Sensor Development
Research Areas
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SEM photo of silicon following laser microtexturing
fig.1 A SEM photo of silicon following laser microtexturing. Courtesy of Harvard University.
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Silicon APD arrays following partial laser texturing
fig. 2 Silicon APD arrays following partial laser texturing

 

Echelle Spectrometer
fig. 3 Echelle Spectrometer
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LIBS Spectrum for Mercury
fig.4 LIBS spectrum for mercury
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fig. 5
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fig. 6a Autocorrelation signal from single dye molecules
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fig. 6b Autocorrelation signal from single dye molecules
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X-ray/Gamma Ray high angular resolution imaging telescope
fig. 7 X-ray/Gamma Ray high angular resolution imaging telescope

 

Images collected at the NASA Marshall Space Flight Center with a scintillator-coupled APD array...
fig. 8 Images collected at the NASA Marshall Space Flight Center with a scintillator-coupled APD array, 125 kVp X-ray source and two FZPs separated by 67 mm.
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16-channel APD tritium probe including readout electronics
fig. 9 16-channel APD tritium probe including readout electronics

 

fig. 10 Laptop powered system for monitoring tritium on surfaces

 

Sensor Development

     The Sensor Development Group advances photonic systems and methods for environmental, industrial and biological sensing applications. Our goal is to promote new scientific discoveries beyond the laboratory and into applications with scientific and commercial benefits.

Research Areas:

Development and use of APDs and APD arrays

Laser Induced Breakdown Spectroscopy (LIBS)
Diffuse Optical Tomography
Laser-based research including LADAR and LIDAR
Polymer based olfactory sensing including landmine detection
Single Molecule Detection for biological applications
Development of radiation imaging instruments

Development and use of APDs and APD arrays

     One of the key focuses of the sensor development group is the use of avalanche photodiode (APD) and APD arrays. Using our in-house fabrication capabilities, we are exploring new applications for these highly sensitive photodetectors. In addition, we continue to explore new fabrication approaches for enhanced wavelength response, speed and sensitivity.

A particular research area of interest has been the enhancement of the near-infrared sensitivity of the APDs. The Advance Sensor engineers have developed a reliable procedure to produce APD arrays with responsivities at 1064 nm over 200 A/W. This is the highest reported responsivity for a silicon-based device at 1064 nm. In collaboration with scientists at Harvard University, this work is made possible by an innovative technique to microtexture the front surface of the APD using high power ultra-short laser pulses (100 fs) (see fig. 1, fig. 2). Using this laser microtexturing a high speed, high gain, low noise APD array sensor module with significantly improved near-IR response was developed. Such an array sensor is an extremely valuable tool for long distance optical communication and for LIDAR/LADAR and other applications.

The Advance sensor group is also evaluating lateral-effect APDs (LEAPs) and quadrant arrays for a range of applications. Using these position-sensitive photodetectors, our work is focused on meeting the requirements of high sensitivity and spatial resolution for long-range optical communications and tracking needs. Additional applications being explored included laser ranging and fluorescent spectroscopy.

See also:

RMD's Quadrant Array Detector

Roughing Up Silicon Improves Near-Infrared Performance - Femtosecond laser helps boost efficiency of avalanche photodiodes. Photonics.com, February, 2007.

Richard A. Myers, Richard Farrell and Arieh M. Karger, "Enhancing Near-IR Avalanche Photodiodes Performance by Femtosecond Laser Microstructuring," Appl. Opt. 45, 8825-8831 (2006).

Laser Induced Breakdown Spectroscopy (LIBS)

RMD's researchers are working on ways to improve upon and utilize laser-induced breakdown spectroscopy (LIBS). LIBS is an extremely simple and powerful tool for stand-off elemental analysis of soil, water and gases. The formation of laser-induced plasma produces a localized blackbody source of atomic emissions. Collection of the plasma's spectral signature with a lens or optical fiber allows examination for elemental components of numerous materials.

Using extremely sensitive Geiger-mode APDs coupled to an echelle spectrometer (fig. 3), RMDs scientist have been exploring ways to make LIBS more commercially viable for analysis on remote platforms. Matching the GPD array format with the output from an echelle spectrometer provides simultaneous monitoring of the major and minor elements of greatest interest, while eliminating the need for a scanning or multiple grating system (fig. 4).

Reference: Richard A. Myers, Arieh M. Karger and David W. Hahn, "Geiger Photodiode Array for Compact, Lightweight Laser-Induced Breakdown Spectroscopy Instrumentation," Appl. Opt. 42, 6072 (2003).

Diffuse Optical Tomography

The area of breast cancer imaging and tumor characterization has experienced rapid growth over the past decade. RMD's scientists are using recent developments in the areas of contrast agents and diffuse optical tomography (DOT) to help bring new clinical technology to market. Our primary target is improvement of breast cancer screening accuracy. Other applications include brain imaging to monitor cerebral function or cerebral hemorrhage, and monitoring tissue and muscle oxygenation.

Researchers in the Advance Sensor group are studying the use of low oxygen content in tumors as a marker of radiation-resistant tumor regions. A laboratory prototype, based on frequency DOT was developed to demonstrate the imaging of luminescent antibody complex with a good resolution in phantom tissues. It employed a near-infrared excitation-detection system using a high gain avalanche photodiodes. We also employed an image reconstruction algorithm developed by our collaborator, Prof. Brian Pogue of Dartmouth College.

Laser-based research including LADAR and LIDAR

The Sensor Development group has a long history of laser-based research ranging from the study and development of novel laser systems to the use of lasers as active components in novel LADAR instrumentation.

Remote sensing systems based upon Light Detection and Ranging (LIDAR) are very promising for standoff detection of various pollution gasses (fig. 5). The advance sensor group at RMD has experimentally demonstrated the capabilities of Raman LIDAR under laboratory conditions and developed the design of a prototype Compact UV Raman LIDAR. The results indicate an excellent ability to identify and quantify the test species. We estimate that the Compact UV Raman LIDAR system will be capable of achieving better than 40 parts-per-million (PPM) sensitivity. Further optical design of a compact UV Raman LIDAR using a linear array of APD, indicated that the smokestack pollution monitoring system will be capable of detecting various pollutants with better than 100 PPM sensitivity at a ranges of 100-200 m. This LIDAR system is expected to result in a variety of commercial environmental monitoring products, including automobile pollution monitoring.

Polymer based olfactory sensing including landmine detection

Scientist in the advance sensor group, in collaboration with research from Tufts University Medical School are working on the development of optical-based olfactory sensors. By integrating a robust and sensitive optical design with newly developed polymer based sensor, targeted odors can be monitored through fluorescence. While a preliminary prototype was assembled for remote sensing of the signature emissions from landmines, clinical applications for early diagnostics of disease are also being pursued.

Single molecule detection and identification instrument and improved substrates for single molecule detection

The Advance Sensor group is exploring ways to improve and utilize instrumentation for single-molecule fluorescence correlation spectroscopy (FCS). Our target application is the study of the detailed behavior of individual molecules in their surroundings. We are exploring instrumentation that employs FCS and two color fluorescence cross-correlation (TC-FCCS) principles in combination with other techniques to increase its usefulness as an analytical tool for studying individual biomolecules. Because a very small number of optical photons are detected from individual molecules, the majority of this work utilizes Geiger-mode APDs (fig. 6a & 6b). In addition, we are working with other scientist and companies to use utilize new nanotechnology for surface-enhancement signals.

Additional single-molecule detection research by the Advance Sensor group includes the designed and implemented of an optical system to study Raman optical activity (ROA) of biomolecules. Using an advanced optical design, we are able to detect signals at the shot noise level to achieve detection of the very weak ROA signals in a relatively compact design. To further utilize the capabilities of this effort, we are seeking ways to further enhance the ROA effects using nanotechnology. Our primary goal for this technology is to elucidate structural and stereochemical information of biomolecules and chiral molecules in general.

Development of radiation imaging instruments

The Advance Sensor group is also involved in the development of radiation imaging systems utilizing RMD's large area APDs and APD arrays. The group has assembled and tested an X-ray/gamma ray imaging telescope for NASA. The telescope consisted of two Fresnel zone plates, a 64-element avalanche photodiode (APD) array coupled to a matching CsI (Tl) scintillator array along with readout electronics and software (fig. 7). Angular resolutions as fine as 30 arc-seconds has been achieved with the prototype system (fig. 8). The development of a compact 64-channel readout unit was a significant feat that has the potential to enable other applications including high-energy physics, scintillating fiber readout, X-ray astronomy, medical imaging, nondestructive testing, LIDAR, LADAR, and laser induced fluorescence.

Reference: Michael R. Squillante, Richard A. Myers, Mitchell Woodring, James F. Christian, Frank Robertson, Ruchard Farrell, Alexander I. Kogan, Timothy Tiernan, and Gerald Entine, "APD-based x-ray imaging telescope using Fresnel zone plates for extremely high resolution," Proc. SPIE 5923, 179-186 (2005).

The Sensor Development group has developed an APD-based probe for monitoring contamination of Tritium (3H) on surfaces (fig. 9). This unit can be operated from the battery power of a laptop computer (fig. 10). A very low energy radiation emitter, tritium is historically very challenging to detect, however, it can be an extremely hazardous material when attached to airborne particles. Facilities at the DOE are in dire need of an improved instrument that can provide them with knowledge of the location and magnitude of tritium contamination prior to decommission and demolition.

Reference: R. Scott Willms, Rick Myers, David Dogrue, and Richard Farrell, "A New Solid State Tritium Surface Monitor," Fusion Science and Technology, 48, 409 (2005).

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